冷軋及退火制備的超細晶粒雙相Mn12Ni2MoTi(Al)鋼
發布人：上海艾荔艾合金股份有限公司www.shailiai.cn
更新時間：2016-06-08
采用 XRD, SEM, TEM, 硬度測試和拉伸實驗研究了冷軋 Mn12Ni2MoTi(Al)鋼經不同工藝退火后的顯微組織及力學性能.
冷軋及退火制備的超細晶粒雙相Mn12Ni2MoTi(Al)鋼AN ULTRAFINE GRAINED DUPLEX Mn12Ni2MoTi(Al) STEEL?FABRICATED BY COLD ROLLING AND ANNEALING采用 XRD, SEM, TEM, 硬度測試和拉伸實驗研究了冷軋 Mn12Ni2MoTi(Al)鋼經不同工藝退火后的顯微組織及力學性能. 結果表明, 馬氏體 Mn12Ni2MoTi(Al)鋼經 65%冷軋及 710~745 ℃退火處理后轉變成主要由奧氏體晶粒和鐵素體晶粒組成的亞微米級超細晶粒雙相組織, 并且彌散分布著第二相析出物顆粒;?在退火中形成的富Ti, Mo及Si的第二相顆粒阻礙了超細再結晶晶粒的粗化, 從而提高了鋼的屈服強度和熱穩定性; 經710 ℃, 24 h長時間退火后, 超細晶粒雙相鋼的平均晶粒尺寸仍然小于500 nm; 超細晶粒雙相鋼延伸率隨室溫奧氏體體積分數增加而增加, 室溫奧氏體體積分數隨退火溫度升高或退火時間延長先增加后降低, 且在745 ℃, 0.5 h 退火時達到最大值. 超細晶粒鋼的屈服強度和總延伸率可達到 900 MPa和 23%以上, 比同種材料淬火馬氏體鋼提高了約一倍。
For decades, transformation induced plasticity (TRIP) assisted steels with high tensile strength and?exceptional ductility at room temperature have attracted a great deal of attentions. Their applications are often?limited due to the low yield strength．In this work, an ultrafine grained (UFG) duplex Mn12Ni2MoTi(Al) TRIP?steel with high yield strength and good ductility is fabricated by cold rolling and subsequent annealing at?710~745 ℃. The microstructure and mechanical properties of the steels with different heat treatment conditions?are investigated by means of XRD, SEM, TEM, hardness and tensile test．It is found that after annealing at?710~745 ℃, the deformation microstructure of the cold-rolled samples has transformed into a sub-micron?ultrafine grained (UFG) duplex microstructure consisting of austenite, ferrite and dispersed second-phase?precipitations. The second-phase precipitations formed during annealing are rich in Ti, Mo and Si, and play an?important role in preventing the ultrafine grains from coarsening, which results in high yield strength and good?thermal stability. After annealing at 710 ℃ for 24 h, the average grain size of the UFG steel is still less than 500?nm. The elongation of the UFG duplex steel is increasing with the increment of the volume fraction of austenite in?the UFG duplex steel at room temperature. The volume fraction of austenite in the UFG duplex steel at room?temperature first increases and then decreases with the annealing temperature and time increasing, and reaches the?maximum value when annealing at 745 ℃ for 0.5 h. The yield strength and total elongation of the UFG steel can?be as large as 900 MPa and 23%, respectively, which are about double those of the quenched martensitic sample.
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