預變形對超高強鋁合金擠壓材組織性能的影響
發布人:上海艾荔艾合金股份有限公司www.shailiai.cn
更新時間:2016-04-01
采用硬度與電導率測試、拉伸試驗、晶間腐蝕和剝落腐蝕試驗以及X射線衍射(XRD)、掃描電鏡(SEM)、電子背散射衍射(EBSD)分析等方法研究預變形對Al-12.45Zn-3.56Mg-1.12Cu-0.21Zr-0.0553Sr鋁合金擠壓材組織與性能的影響。
預變形對超高強鋁合金擠壓材組織性能的影響Effect of pre-deformation on microstructure and properties of ultra-high strength aluminum alloy extrusion materials采用硬度與電導率測試、拉伸試驗、晶間腐蝕和剝落腐蝕試驗以及X射線衍射(XRD)、掃描電鏡(SEM)、電子背散射衍射(EBSD)分析等方法研究預變形對Al-12.45Zn-3.56Mg-1.12Cu-0.21Zr-0.0553Sr鋁合金擠壓材組織與性能的影響。結果表明:該合金在(121 ℃, 24 h)時效制度下,預變形處理能有效引入位錯,位錯密度從0.197×10-14 m-2提高到1.156×10-14 m-2;同時,由于位錯對強度的貢獻高達58.7 MPa。根據EBSD分析,經預變形處理后,合金的低角度晶界所占比例為66.2%,比未經預變形處理的合金提高12.6%,平均晶界角度值降低3.894°,平均晶粒尺寸增長6.396 mm。預變形能夠明顯提高合金的抗晶間腐蝕性能(最大晶間腐蝕深度由222.1 mm降低至165 mm),對剝落腐蝕性能的影響不明顯。
The effects of pre-deformation on microstructure and properties of Al-12.45Zn-3.56Mg-1.12Cu-0.21Zr- 0.0553Sr ultra-high strength aluminum alloy extrusion materials were studied by means of micro-hardness tester and electrical conductivity test, tensile test, intergranular and exfoliation corrosion experiment, X-ray diffraction (XRD), scanning electron microscopy (SEM) and electron back-scattered diffraction (EBSD) analysis. The results show that in the aging system at 121 ℃ for 24 h, the pre-deformation can effectively introduce dislocations,the dislocation density increases from 0.197×10-14 m-2to 1.156×10-14 m-2, and the strength reaches up to 58.7 MPa because of the dislocation contribution.Based on EBSD analysis, after pre-deformation treatment, the low angle grain boundary proportion (66.2%) of the pre-deformation alloy increases by 12.6% than that of the underformed alloy, the mean misorientation value reduces 3.894°, and the average grain size increases by 6.396 μm. The pre-deformation treatment can significantly improve the intergranular corrosion resistance properties (the maximum intergranular corrosion depth reducing from 222.1 μm to 165 μm), but little improvement on exfoliation corrosion performance.
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